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Ciproxin 200 ug/ml (0.02%) and 5-chloro-2,4-dimen-2-en-1-ol (0.1%) in the same mixture, mixture was stirred for 30 min at 37°C. 3H nM of 4-(4-fluorobenzyloxy)-1,2,3,4-tetramethyl-4H-8-oxo-1,2,3,4-tetrahydrobenzene, 4-fluorobenzyloxy-2-pyrrolidin-1-ylidene (40 mg), and ethyl alcohol (10 ml) were added. The mixture was stirred for 2 h at 22°C, and the reaction mixture was cooled and evaporated to dryness. The residue was purified by silica gel column chromatography (ethyl acetate/n-hexane=30:70) to give a blue oil of racemic mixture 2-fluoro-N-[4-(4-fluorobenzyloxy)-1,2,3,4-tetramethyl-4H-8-oxo-1,2,3,4-tetrahydrobenzene] and 1-(4-fluorobenzyloxy)-N-[4-(4-fluorobenzyloxy)-1,2,3,4-tetramethyl-4H-8-oxo-1,2,3,4-tetrahydrobenzene]. The crude racemic mixture of 2-fluoro-2-pyrrolidin-1-ylidene (50 mg) and 1,2,3,4-tetramethyl-4H-8-oxo-1,2,3,4-tetrahydrobenzene (10 was dissolved in ethanol (50 ml) and the mixture was stirred for 1 adderall for adhd in adults h at 4°C to prevent precipitation of the 2-fluoro-4-hydroxy-1,2,3,4- tetrahydrobenzene intermediate. mixture was cooled and evaporated to dryness. The residue was purified by alumina flotation chromatography (ethyl acetate/n-hexane=50:50) to give the title compound as a colorless oil. EXAMPLE 9 N-[4-(4-fluorobenzyloxy)-1,2,3,4-tetramethyl-4H-8-oxo-1,2,3,4-tetrahydrobenzene] (100 mg) was combined with a solution of 4-fluoro-N-[4-(4-fluorobenzyloxy)-1,2,3,4-tetramethyl-4H-8-oxo-1,2,3,4-tetrahydrobenzene] (20 mg) in DMSO (60 ml) and ethanol (200 was added. The mixture stirred at room temperature for 1 h. The mixture was poured into cold water. The solution was extracted with ethyl acetate (100 ml) and the residue was purified by silica gel eluting with a saturated aqueous sodium chloride solution (20 ml, 1 M) to give the title compound as a colorless oil (100 mg, 42%). The crude racemic mixture of (100 mg) and 1,2,3,4-tetramethyl-4H-8-oxo-1,2,3,4-tetrahydrobenzene (20 was dissolved in ethanol (50 ml) and the mixture was stirred at room temperature for 1 h. The mixture was poured into cold water. The solution was extracted with ethyl acetate (100 ml) and the residue was purified by silica gel eluting with a saturated aqueous sodium chloride solution (20 ml, 1 adderall good for bipolar M) to give the title compound as a colorless oil (100 mg, 42%). EXAMPLE 10 A mixture of 3-(dimethylamino)-1,2,3,4-tetrahydrobenzene (20 mg) in aqueous ammonia ml) was diluted in THF (20 ml). The mixture was stirred for 1 h at room temperature. Then 0.2 M aqueous hydrochloric acid was added and the mixture stirred for 1 h at room temperature. The acid solution was extracted with hexane (100 ml). The extracts were washed with water (40 ml), brine (2×10 ml) and dried over anhydrous sodium sulfate. The extracts were concentrated under reduced pressure to afford a crude aqueous solution of the compound in hexane (100 ml, 20%). The residue was purified by column chromatography.

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